zhpsЖурнал прикладной спектроскопииZhurnal Prikladnoii Spektroskopii0514-7506B. I. Stepanov Institute of Physics of the National Academy of Scienceszhps-614Research ArticleСтатьиОСЛАБЛЕНИЕ ФЛУОРЕСЦЕНЦИИ ПОЧЕЧНЫХ КАМНЕЙ В СПЕКТРОСКОПИИ КОМБИНАЦИОННОГО РАССЕЯНИЯ СВЕТА С ПОМОЩЬЮ ХИМИЧЕСКОГО ОТБЕЛИВАНИЯFLUORESCENCE REDUCTION IN RAMAN SPECTROSCOPY BY CHEMICAL BLEACHING ON RENAL STONESKocademirM.KocademirM.

34134, Стамбул

Science Faculty, Physics Department, Vezneciler

34134 Istanbul

KumruM.KumruM.

79106, Фрайбург

Faculty of Medicine, Department of Urology

79106 Freiburg

GölcükK.GölcükK.

53127, Бонн, Германия

53127 Bonn

Suarez-IbarrolaR.Suarez-IbarrolaR.

79106, Фрайбург

Faculty of Medicine, Department of Urology

79106 Freiburg

MiernikА.MiernikA.

79106, Фрайбург

Faculty of Medicine, Department of Urology

79106 Freiburg

Стамбульский университет, ВезнеджилерIstanbul UniversityФрайбургский университет, медицинский центрUniversity of Freiburg – Medical CenterИнститут экспериментальной эпилептологии и исследований познания, Боннский университетInstitute of Experimental Epileptology and Cognition Research, University of Bonn Medical Center Life and Brain202007052020872268274Copyright © Kocademir M., Kumru M., Gölcük K., Suarez-Ibarrola R., Miernik А., 20202020Kocademir M., Kumru M., Gölcük K., Suarez-Ibarrola R., Miernik А.Kocademir M., Kumru M., Gölcük K., Suarez-Ibarrola R., Miernik A.Данная работа распространяется под лицензией Creative Commons Attribution 4.0.This work is licensed under a Creative Commons Attribution 4.0 License.https://zhps.ejournal.by/jour/article/view/614

Метод химического отбеливания с помощью пероксида водорода применен к почечным камням двух различных типов. После процесса отбеливания осуществлена характеризация. Камни идентифицированы как фосфат кальция и моногидрат оксалата кальция. Образцы проанализированы с помощью дисперсионной КР-спектроскопии с λ возб = 532 нм. Для сравнения результатов образцы измерены с помощью ИК-Фурье- и КР-Фурье-спектроскопии. Отношение минерал/матрица для полос КР изменилось для обоих образцов, однако без каких-либо заметных сдвигов частоты в спектрах КР.

In this study, a hydrogen peroxide-based chemical bleaching technique was applied on two different types of renal stones. The characterization was achieved after the bleaching process. They were identified as calcium phosphate and calcium oxalate monohydrate. The samples were analyzed using dispersive Raman spectroscopy with a 532 nm excitation laser. To compare the results, the samples were measured using both FT-IR and FT-Raman spectroscopy. Consequently, the mineral/matrix ratio of Raman bands changed for both samples, but without any noticeable frequency shifts in the Raman spectra.

спектроскопия комбинационного рассеяния светауменьшение флуоресценциихимическое отбеливаниепочечный каменьфосфат кальцияоксалат кальцияRaman spectroscopyfluorescence reductionchemical bleachingrenal stonecalcium phosphatecalcium oxalateReferencesV. Mazet, C. Carteret, D. Brie, J. Idier, B. Humbert, Chemometr. Intell. Lab. Syst., 76, 121–133 (2005).V. Mazet, C. Carteret, D. Brie, J. Idier, B. Humbert, Chemometr. Intell. Lab. Syst., 76, 121–133 (2005).A. P. Shreve, N. J. Cherepy, R. A. Mathies, Appl. Spectrosc., 46, 707–711 (1992).A. P. Shreve, N. J. Cherepy, R. A. Mathies, Appl. Spectrosc., 46, 707–711 (1992).S. Yang, B. Li, M. N. Slipchenko, A. Akkus, N. G. Singer, Y. N. Yeni, O. Akkus, J. Raman Spectrosc., 44, 1089–1095 (2013).S. Yang, B. Li, M. N. Slipchenko, A. Akkus, N. G. Singer, Y. N. Yeni, O. Akkus, J. Raman Spectrosc., 44, 1089–1095 (2013).Y. K. Min, T. Yamamoto, E. Kohda, T. Ito, H. Hamaguchi, J. Raman Spectrosc., 36, 73–75 (2005).Y. K. Min, T. Yamamoto, E. Kohda, T. Ito, H. Hamaguchi, J. Raman Spectrosc., 36, 73–75 (2005).M. Sauer, J. Hofkens, J. Enderlein, Handbook of Fluorescence Spectroscopy and Imaging, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Germany (2015); doi: 10.1002/9783527633500.ch1.M. Sauer, J. Hofkens, J. Enderlein, Handbook of Fluorescence Spectroscopy and Imaging, Wiley-VCH Verlag GmbH & Co. KGaA, Weinheim, Germany (2015); doi: 10.1002/9783527633500.ch1.D. Wei, S. Chen, Q. Liu, Appl. Spectrosc. Rev., 50, N 5, 387–406 (2015).D. Wei, S. Chen, Q. Liu, Appl. Spectrosc. Rev., 50, N 5, 387–406 (2015).T. C. Chen, D. A. Shea, M. D. Morris, Appl. Spectrosc., 56, 1035–1037 (2002).T. C. Chen, D. A. Shea, M. D. Morris, Appl. Spectrosc., 56, 1035–1037 (2002).J. R. Ferraro, K. Nakamoto, Ch. W. Brown, Introductory Raman Spectroscopy, 2 nd ed., Academic Press, San Diego (2003).J. R. Ferraro, K. Nakamoto, Ch. W. Brown, Introductory Raman Spectroscopy, 2 nd ed., Academic Press, San Diego (2003).V. Košarová, D. Hradil, I. Nemec, P. Bezdicka, V. Kanický, J. Raman Spectrosc., 44, 1570–1577 (2013).V. Košarová, D. Hradil, I. Nemec, P. Bezdicka, V. Kanický, J. Raman Spectrosc., 44, 1570–1577 (2013).P. J. Cadusch, M. M. Hlaing, S. A. Wade, S. L. McArthur, P. R. Stoddart, J. Raman Spectrosc., 44, 1587–1595 (2013).P. J. Cadusch, M. M. Hlaing, S. A. Wade, S. L. McArthur, P. R. Stoddart, J. Raman Spectrosc., 44, 1587–1595 (2013).G. Schulze, A. Jirasek, M. M. L. Yu, A. Lim, R. F. B. Turner, M. W. Blades, Appl. Spectrosc., 59, 545–574 (2005).G. Schulze, A. Jirasek, M. M. L. Yu, A. Lim, R. F. B. Turner, M. W. Blades, Appl. Spectrosc., 59, 545–574 (2005).Handbook of Vibrational Spectroscopy, Eds. N. Sheppard, J. M. Chalmers, P. R. Griffiths, Vol. 1, John Wiley and Sons, Chichester, 1–32 (2002).Handbook of Vibrational Spectroscopy, Eds. N. Sheppard, J. M. Chalmers, P. R. Griffiths, Vol. 1, John Wiley and Sons, Chichester, 1–32 (2002).K. Golcuk, G. S. Mandair, A. F. Callender, N. Sahar, D. H. Kohn, M. D. Morris, Biochim. Biophys. Acta, 1758, 868–873 (2006).K. Golcuk, G. S. Mandair, A. F. Callender, N. Sahar, D. H. Kohn, M. D. Morris, Biochim. Biophys. Acta, 1758, 868–873 (2006).D. A. Shea, M. D. Morris, Appl. Spectrosc., 56, 182–186 (2002).D. A. Shea, M. D. Morris, Appl. Spectrosc., 56, 182–186 (2002).G. Penel, G. Leroy, E. Bre’s, Appl. Spectrosc., 52, 312–313 (1998).G. Penel, G. Leroy, E. Bre’s, Appl. Spectrosc., 52, 312–313 (1998).K. Moharamzadeh, Biocompatibility of Dental Biomaterials, Woodhead Publishing Series in Biomaterials, 113–129 (2017).K. Moharamzadeh, Biocompatibility of Dental Biomaterials, Woodhead Publishing Series in Biomaterials, 113–129 (2017).T. Vargas-Koudriavtsev, R. Durán-Sedó, P. Sáenz-Bonilla, V. Bonilla-Mora, M. Guevara-Bertsch, R. Antonio Jiménez-Corrales, O. A. Herrera-Sancho, Rev. Odontol. Mex., 19, 228–235 (2015).T. Vargas-Koudriavtsev, R. Durán-Sedó, P. Sáenz-Bonilla, V. Bonilla-Mora, M. Guevara-Bertsch, R. Antonio Jiménez-Corrales, O. A. Herrera-Sancho, Rev. Odontol. Mex., 19, 228–235 (2015).M. Unal, O. Akkus, Bone, 81, 315–326 (2015).M. Unal, O. Akkus, Bone, 81, 315–326 (2015).G. S. Mandair, M. D. Morris, Bonekey Rep., 4, 1–8 (2015).G. S. Mandair, M. D. Morris, Bonekey Rep., 4, 1–8 (2015).H. J. Butler, L. Ashton, B. Bird, G. Cinque, K. Curtis, J. Dorney, W. K. Esmonde, N. J. Fullwood, B. Gardner, P. L. M. Hirsch, M. J. Walsh, M. R. M. Ainsh, N. Stone, F. L. Martin, Nature Protocol, 11, 664–687 (2016).H. J. Butler, L. Ashton, B. Bird, G. Cinque, K. Curtis, J. Dorney, W. K. Esmonde, N. J. Fullwood, B. Gardner, P. L. M. Hirsch, M. J. Walsh, M. R. M. Ainsh, N. Stone, F. L. Martin, Nature Protocol, 11, 664–687 (2016).J. M. Silveira, S. Longelin, A. D. Mataa, M. L. Carvalho, J. Raman Spectrosc., 43, 1089–1093 (2012).J. M. Silveira, S. Longelin, A. D. Mataa, M. L. Carvalho, J. Raman Spectrosc., 43, 1089–1093 (2012).Z. Li1, M. AI-Jawad, S. Siddiqui, J. D. Pasteris, Sci. Rep., 5, 1–10 (2015).Z. Li1, M. AI-Jawad, S. Siddiqui, J. D. Pasteris, Sci. Rep., 5, 1–10 (2015).M. Ritza, L. Vaculíkovác, J. Kupkováe, E. Plevovác, L. Bartonováa, Vibr. Spectrosc., 84, 7–15 (2016).M. Ritza, L. Vaculíkovác, J. Kupkováe, E. Plevovác, L. Bartonováa, Vibr. Spectrosc., 84, 7–15 (2016).J. J. Freeman, B. Wopenka, M. J. Silva, J. D. Pasteris, Calcif. Tissue Int., 68, 156–162 (2001).J. J. Freeman, B. Wopenka, M. J. Silva, J. D. Pasteris, Calcif. Tissue Int., 68, 156–162 (2001).M. D. Morris, G. S. Mandair, Clin. Orthopaed. Relat. Res., 469, 2160–2169 (2011).M. D. Morris, G. S. Mandair, Clin. Orthopaed. Relat. Res., 469, 2160–2169 (2011).S. K. H. Khalil, M. A. Azooz, J. Appl. Sci. Res., 3, 387–391 (2007).S. K. H. Khalil, M. A. Azooz, J. Appl. Sci. Res., 3, 387–391 (2007).M. Daudon, M. F. Protat, R. J. Reveillaud, H. Jaeschke-Boyer, Kidney Int., 23, 842–850 (1983).M. Daudon, M. F. Protat, R. J. Reveillaud, H. Jaeschke-Boyer, Kidney Int., 23, 842–850 (1983).M. Pucetaite, M. Velicka, S. Tamosaityte, V. Sablinskas, Plasmonic Biol. Med., 8957, 1–8 (2014).M. Pucetaite, M. Velicka, S. Tamosaityte, V. Sablinskas, Plasmonic Biol. Med., 8957, 1–8 (2014).E. E. Lawson, B. W. Barry, A. C. Williams, H. G. M. Edwards, J. Raman Spectrosc., 28, 111–117 (1997).E. E. Lawson, B. W. Barry, A. C. Williams, H. G. M. Edwards, J. Raman Spectrosc., 28, 111–117 (1997).C. Paluszkiewicz, M. Gałka, W. Kwiatek, A. Parczewski, S. Walas, Biospectroscopy, 3, 403–407 (1997).C. Paluszkiewicz, M. Gałka, W. Kwiatek, A. Parczewski, S. Walas, Biospectroscopy, 3, 403–407 (1997).C. G. Kontoyannis, N. C. Bouropoulos, P. G. Koutsoukos, Appl. Spectrosc., 51, 64–67 (1997).C. G. Kontoyannis, N. C. Bouropoulos, P. G. Koutsoukos, Appl. Spectrosc., 51, 64–67 (1997).R. Selvaraju, G. Thiruppathi, A. Raja, Spectrochim. Acta, A, 93, 260–265 (2012).R. Selvaraju, G. Thiruppathi, A. Raja, Spectrochim. Acta, A, 93, 260–265 (2012).M. H. Khaskheli, S. T. H. Sherazi, H. M. Ujan, S. A. Mahesar, Turk. J. Chem., 36, 477–483 (2012).M. H. Khaskheli, S. T. H. Sherazi, H. M. Ujan, S. A. Mahesar, Turk. J. Chem., 36, 477–483 (2012).X. Carpentier, M. Daudon, O. Traxer, P. Jungers, A. Mazouyes, G. Matzen, E. Véron, D. Bazin, Urology, 73, 968–975 (2009).X. Carpentier, M. Daudon, O. Traxer, P. Jungers, A. Mazouyes, G. Matzen, E. Véron, D. Bazin, Urology, 73, 968–975 (2009).R. Selvaraju, A. Raja, G. Thiruppathi, Spectrochim. Acta, A, 137, 1397–1402 (2015).R. Selvaraju, A. Raja, G. Thiruppathi, Spectrochim. Acta, A, 137, 1397–1402 (2015).E. L. Prien, E. L. Prien, Am. J. Med., 45, 654–672 (1968).E. L. Prien, E. L. Prien, Am. J. Med., 45, 654–672 (1968).S. Matsuzaki, K. Matsuzaki, T. Tanikawa, A. Masuda, F. Matsunaga, Int. J. Urol., 2, 235–237 (1995).S. Matsuzaki, K. Matsuzaki, T. Tanikawa, A. Masuda, F. Matsunaga, Int. J. Urol., 2, 235–237 (1995).Y. H. Lee, W. C. Huang, J. Y. Tsai, J. K. Huang, J. Urol., 161, 1453–1457 (1999).Y. H. Lee, W. C. Huang, J. Y. Tsai, J. K. Huang, J. Urol., 161, 1453–1457 (1999).E. V. Wilson, M. J. Bushirib, V. K. Vaidyan, Spectrochim. Acta, A, 77, 442–445 (2010).E. V. Wilson, M. J. Bushirib, V. K. Vaidyan, Spectrochim. Acta, A, 77, 442–445 (2010).H. T. H. Shing, S. L. Yang, C. L. Cheng, W. T. Cheng, Urol. Res., 39, 165–170 (2011).H. T. H. Shing, S. L. Yang, C. L. Cheng, W. T. Cheng, Urol. Res., 39, 165–170 (2011).M. Kocademir, A. Baykal, M. Kumru, M. L. Tahmaz, Spectrochim. Acta, A, 160, 1–7 (2016).M. Kocademir, A. Baykal, M. Kumru, M. L. Tahmaz, Spectrochim. Acta, A, 160, 1–7 (2016).M. Serkan Yalçın, Mesut Tek, J. Appl. Spectrosc., 85, 61050–61057 (2019).M. Serkan Yalçın, Mesut Tek, J. Appl. Spectrosc., 85, 61050–61057 (2019).S. R. Khan, P. N. Shevock, R. L. Hackett, Calcif. Tissue Int., 42, 91–96 (1988).S. R. Khan, P. N. Shevock, R. L. Hackett, Calcif. Tissue Int., 42, 91–96 (1988).S. Sandersius, P. Rez, Urol. Res., 35, 287–293 (2007).S. Sandersius, P. Rez, Urol. Res., 35, 287–293 (2007).H. Tsuda, J. A. Materia, J. Dent. Res., 73, 1703–1710 (1994).H. Tsuda, J. A. Materia, J. Dent. Res., 73, 1703–1710 (1994).

The authors declare that there are no conflicts of interest present.