IR-SPECTROSCOPIC METHOD FOR DETERMINING THE DEGREE OF NITRATION OF β-CYCLODEXTRIN
Abstract
An IR-spectroscopic technique for determining the degree of nitration of b-cyclodextrin has been elaborated. It permits to determine the total number of ONO2-groups in partial b-cyclodextrin nitrates. The relative error of the measurement of the proposed method is 2%. The measurement range for the degree of nitration is from 33 to 100% of nitrate groups per the β-cyclodextrin molecule.
About the Authors
M. D. Rodin
Institute of Problems of Chemical Physics of the Russian Academy of Sciences; Lomonosov Moscow State University
Russian Federation
Russian Federation
L. B. Romanova
Institute of Problems of Chemical Physics of the Russian Academy of Sciences
Russian Federation
Russian Federation
A. V. Darovskih
Institute of Problems of Chemical Physics of the Russian Academy of Sciences
Russian Federation
Russian Federation
M. A. Gorbunova
Institute of Problems of Chemical Physics of the Russian Academy of Sciences
Russian Federation
Russian Federation
A. E. Tarasov
Institute of Problems of Chemical Physics of the Russian Academy of Sciences
Russian Federation
Russian Federation
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Review
For citations:
Rodin M.D., Romanova L.B., Darovskih A.V., Gorbunova M.A., Tarasov A.E. IR-SPECTROSCOPIC METHOD FOR DETERMINING THE DEGREE OF NITRATION OF β-CYCLODEXTRIN. Zhurnal Prikladnoii Spektroskopii. 2018;85(4):639-644. (In Russ.)
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