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Microstructure and Optical Characteristics of Nickel Nanoparticles Obtained by One-Step Synthesis Method
Abstract
Nickel nanoparticles were synthesized at room temperature by a one-step method of chemical reduction of Ni ions from nickel chloride hexahydrate (NiCl2 · 6H2O) using sodium tetrahydride borate (NaBH4). The microstructure of nanoparticles was studied by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. Analysis of X-ray diffraction and Raman spectroscopy data showed that the resulting nanoparticles have a cubic structure of metallic nickel with a crystallite size (coherent scattering region) in the range of 3–6 nm. Morphology studies indicate that nickel nanoparticles are spherical in shape and are in contact with each other, forming large agglomerates of nanograins.
About the Authors
V. F. Gremenok
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science;
Belarusian State University of Informatics and Radioelectronics
Беларусь
Беларусь
Minsk
N. N. Musaeva
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Азербайджан
Азербайджан
Baku
Kh. Kh. Khalilova
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Азербайджан
Азербайджан
Baku
A. L. Zheludkevich
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science
Беларусь
Беларусь
Minsk
O. F. Demidenko
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science
Беларусь
Беларусь
Minsk
D. A. Kiselev
National Research Technological University “MISIS”
Россия
Россия
Moscow
V. V. Khoroshko
Belarusian State University of Informatics and Radioelectronics
Беларусь
Беларусь
Minsk
B. M. Izzatov
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Азербайджан
Азербайджан
Baku
M. T. Alizade
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Азербайджан
Азербайджан
Baku
References
1. S. Shan, J. Luo, N. Kang, J. Wu, W. Zhao, H. Cronk, C.-J. Zhong. Modeling, Characterization, and Production of Nanomaterials, Woodhead Publishing Series in Electronic and Optical Materials (2015) 253—288
2. D. Astruc. Chem. Rev., 120 (2020) 461—463
3. N. D. Klein, K. R. Hurley, Z. V. Feng, C. L. Haynes. Anal. Chem., 87 (2015) 4356—4362
4. M. Fadlallah, A. G. Abdelrahman, U. Schwingenschlogl, A. A. Maarouf. Nanotechnology, 30, N 8 (2019) 085709(1—25)
5. T. Kamal, S. B. Khan, A. M. Asiri. Environ. Poll., 218 (2016) 625—633
6. T. Matsuo, M. Ueki, M. Takeyama, R. Tanaka. J. Mater. Sci., 22 (1987) 1901—1907
7. N. D. Jaji, B. H. Othman, H. L. Lee, M. H. Hussin, D. Hui. Nanotechnol. Rev., 10, N 1 (2021) 318—329
8. Y. X. Gan, A. H. Jayatissa, Z. Yu, X. Chen, M. Li. J. Nanomaterials, 2020 (2020) 1—3
9. G. G. Couto, J. J. Klein, W. H. Schreiner, D. H. Mosca, A. J. A. Oliveira, A. J. G. Zarbin. J. Colloid and Interface Sci., 311 (2007) 461—468
10. Z. Ying, J. Shengming, Q. Guanzhou, Y. Min. Mater. Sci. and Eng., B122 (2005) 222—225
11. S.-H. Wu, D.-Y. Chen. J. Colloid and Interface Sci., 259 (2003) 282—286 [12] P. Scherrer. Göttinger Nachrichten Gesell., 2 (1918) 98
12. A. Patterson. Phys. Rev., 56, N 10 (1936) 978—982
13. G. Williamson, W. Hall. Acta Metallurgica, 1 (1953) 22—31
14. M. Ali, N. Remalli, V. Gedela, B. Padya, P. K. Jain, A. Al-Fatesh, U. A. Rana, V. V. S. S. Srikanth. Solid State Sci., 64 (2017) 34—40
15. D. L. Andrews, A. A. Demidov. An Introduction to Laser Spectroscopy, Springer Science+Business Media, LLC, Springer, Boston, MA (2002) 77—104
16. R. E. Dietz, W. F. Brinkman, A. E. Mexiner, H. J. Guggenheim. Phys. Rev. Lett., 27 (1971) 814—817
17. D. Kumar, H. Singh, S. Banerjee. Adv. Sci. Eng. Med., 8 (2016) 1—11
18. N. Mironova-Ulmane, A. Kuzmin, I. Steins, J. Grabis, I. Sildos. J. Physics: Conf. Ser., 93 (2007) 012039(1—5)
19. H. C. Choi, Y. M. Yung, S. B. Kim. Vibr. Spectrosc., 37, N 1 (2005) 33—38
20. М. В. Кузнецов, А. В. Сафонов, Д. А. Бобрешов, О. В. Белоусова, Ю. Г. Морозов. Наноструктурированные материалы и функциональные покрытия, № 1 (2020) 65—74 [M. V. Kuznetsov, A. V. Safonov, D. A. Bobreshov, O. V. Belousova, I. G. Morozov. Poroshkovaya Metallurgiya i Funktsional’nye Pokrytiya (Universities’ Proceedings. Powder Metallurgy and Functional Coatings), N 1 (2020) 65—74]
21. K. C. Patil, M. S. Hegde, T. Rattan, S. T. Aruna. Chemistry of Nanocrystalline Oxide Materials. Combustion Synthesis, Properties and Applications, World Scientific Publishing Co., New Jersey (2008) 154—178
Review
For citations:
Gremenok V.F., Musaeva N.N., Khalilova Kh.Kh., Zheludkevich A.L., Demidenko O.F., Kiselev D.A., Khoroshko V.V., Izzatov B.M., Alizade M.T. Microstructure and Optical Characteristics of Nickel Nanoparticles Obtained by One-Step Synthesis Method. Zhurnal Prikladnoii Spektroskopii. 2024;91(3):417-422. (In Russ.)
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