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Microstructure and Optical Characteristics of Nickel Nanoparticles Obtained by One-Step Synthesis Method
Abstract
Nickel nanoparticles were synthesized at room temperature by a one-step method of chemical reduction of Ni ions from nickel chloride hexahydrate (NiCl2 · 6H2O) using sodium tetrahydride borate (NaBH4). The microstructure of nanoparticles was studied by X-ray diffraction, Raman spectroscopy, scanning and transmission electron microscopy. Analysis of X-ray diffraction and Raman spectroscopy data showed that the resulting nanoparticles have a cubic structure of metallic nickel with a crystallite size (coherent scattering region) in the range of 3–6 nm. Morphology studies indicate that nickel nanoparticles are spherical in shape and are in contact with each other, forming large agglomerates of nanograins.
About the Authors
V. F. Gremenok
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science;
Belarusian State University of Informatics and Radioelectronics
Belarus
Belarus
Minsk
N. N. Musaeva
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Azerbaijan
Azerbaijan
Baku
Kh. Kh. Khalilova
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Azerbaijan
Azerbaijan
Baku
A. L. Zheludkevich
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science
Belarus
Belarus
Minsk
O. F. Demidenko
Scientific and Practical Center of the National Academy of Sciences of Belarus for Materials Science
Belarus
Belarus
Minsk
D. A. Kiselev
National Research Technological University “MISIS”
Russian Federation
Russian Federation
Moscow
V. V. Khoroshko
Belarusian State University of Informatics and Radioelectronics
Belarus
Belarus
Minsk
B. M. Izzatov
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Azerbaijan
Azerbaijan
Baku
M. T. Alizade
Institute of Physics Ministry of Science and Education of the Republic of Azerbaijan
Azerbaijan
Azerbaijan
Baku
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Review
For citations:
Gremenok V.F., Musaeva N.N., Khalilova Kh.Kh., Zheludkevich A.L., Demidenko O.F., Kiselev D.A., Khoroshko V.V., Izzatov B.M., Alizade M.T. Microstructure and Optical Characteristics of Nickel Nanoparticles Obtained by One-Step Synthesis Method. Zhurnal Prikladnoii Spektroskopii. 2024;91(3):417-422. (In Russ.)
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