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Spectral Analysis of Glycyrrhizic Acid, Lagochilin, Lagochirzine and Their Derivatives
Abstract
The two-dimensional NMR spectroscopy method was used to assign signals of hydrogen and carbon atoms in glycyrrhizic acid, monoammonium salt of glycyrrhizic acid, lagochirsine, lagochilin, its tetraacetyl and isopropylidene derivatives in various solvents. The compounds were studied by tandem mass spectrometry in modes ESI and APCI.
About the Authors
A. V. Baranovsky
Institute of Bioorganic Chemistry of the National Academy of Sciences of Belarus
Belarus
Belarus
Minsk
S. N. Sokolov
Institute of Bioorganic Chemistry of the National Academy of Sciences of Belarus
Belarus
Belarus
Minsk
S. A. Fatykhava
Institute of Bioorganic Chemistry of the National Academy of Sciences of Belarus
Belarus
Belarus
Minsk
P. S. Shabunya
Institute of Bioorganic Chemistry of the National Academy of Sciences of Belarus
Belarus
Belarus
Minsk
R. S. Esanov
Institute of Bioorganic Chemistry of the Academy of Sciences of the Republic of Uzbekistan
Uzbekistan
Uzbekistan
Tashkent
F. N. Tashpulatov
Institute of Bioorganic Chemistry of the Academy of Sciences of the Republic of Uzbekistan
Uzbekistan
Uzbekistan
Tashkent
A. D. Matchanov
Institute of Bioorganic Chemistry of the Academy of Sciences of the Republic of Uzbekistan
Uzbekistan
Uzbekistan
Tashkent
References
1. C. Fiore, M. Eisenhut, E. Ragazzi, G. Zanchin, D. Armanini. J. Ethnopharmacol., 99, N 3 (2005) 317—324, https://doi.org/10.1016/j.jep.2005.04.015
2. E. E. Tykarska, Z. Dutkiewicz, D. Baranowski, Z. Gdaniec, M. Gdaniec. Cryst. Growth and Design, 14, N 11 (2014) 5871—5880, https://doi.org/10.1021/cg5010962
3. S. S. Petrova, A. A. Schlotgauer, A. I. Kruppa, T. V. Leshina. Z. Phys. Chem., 231, N 4 (2016) 839—855, https://doi.org/10.1515/zpch-2016-0845
4. N. E. Polyakov, V. K. Khan, M. B. Taraban, T. V. Leshina, N. F. Salakhutdinov, G. A. Tolstikov. J. Phys. Chem. B, 109 (2005) 24526—24530, https://doi.org/10.1021/jp053434v
5. Ф. А. Собирова, А. Х. Исламов, Л. К. Элмуродов, А. Х. Расулов, З. А. Собирова, Г. Н. Артикова, А. Д. Матчанов. Химия растит. сырья, № 1 (2022) 123—132, https://doi.org/10.14258/jcprm.2022017757
6. L. Yu. Izotova, S. A. Talipov, B. T. Ibragimov, B. Bekbulatova, R. Islamov, U. N. Zainutdinov. Chem. Nat. Compd., 36, N 2 (2000) 181—184, https://doi.org/10.1007/BF02236426
7. U. N. Zainutdinova, M. P. Pulatova, T. A. Badalbaeva, R. U. Umarova, Z. I. Mavlyankulova, T. P. Pulatova, Kh. A. Aslanova. Chem. Nat. Compd., 30, N 1 (1994) 27—29, https://doi.org/10.1007/BF00638413
8. А. Д. Матчанов, А. М. Усуббаев, Б. М. Бекпулатова, М. О. Давлатбоева, Р. С. Эсанов. Евразийский журн. мед. и естеств. наук, 4, № 2 (Special Issue) (2024) 193—195, https://in-academy.uz/index.php/EJMNS/article/view/27784
9. N. N. Gibadullina, L. A. Yakovishin, V. I. Grishkovets, L. V. Spirikhin, V. A. Vakhitov, D. V. Ishmetova, V. A. Dokichev. Russ. Chem. Bull., 73, N 1 (2024) 179—188, https://doi.org/10.1007/s11172-024-4130-0
10. Zhao Yanyan, Liu Liyan, Han Yuanyuan, Wang Yan, Shi Minjian, Zhongguo Yiyao, Gongye Zazhi. Chin. J. Pharm., 45, N 7 (2014) 663—670, http://www.cjph.com.cn/EN/Y2014/V45/I7/663
11. A. D. Matchanov, D. N. Dalimov, U. N. Zainutdinov, N. L. Vypova, A. Kh. Islamov, B. M. Bekpolatova. Chem. Nat. Compd., 53, N 4 (2017) 665—669, https://doi.org/10.1007/s10600-017-2086-0
12. Venkata Sai, Prakash Chaturvedula, Oliver Yu, Guohong Mao. Eur. Chem. Bull., 3, N 1 (2014) 104— 107, http://epa.niif.hu/02200/02286/00023/pdf/EPA02286_european_chemical_bulletin_2014_01_104-107.pdf
13. L. A. Baltina, O. Kunert, A. A. Fatykhov, R. M. Kondratenko, L. V. Spirikhin, L. A. Baltina, Jr., F. Z. Galin, G. A. Tolstikov, E. Haslinger. Chem. Nat. Compd., 41, N 4 (2005) 432—435, https://doi.org/10.1007/s10600-005-0171-2
14. G. G. Zapesochnaya, E. N. Zvonkova, V. A. Kurkin, E. V. Kazakova, L. N. Pervykh, B. I Sheichenko, V. A. Bykov. Chem. Nat. Comp., 30, N 6 (1994) 720—726, https://doi.org/10.1007/BF00630611
15. Yasumasa Yamada, Atsuko Nakamura, Kiyoko Yamamoto, Hiroe Kikuzaki. Biosci. Biotech. Biochem., 58, N 2 (1994) 436—437, https://doi.org/10.1271/bbb.58.436
16. Y.-F. Zheng, L.-W. Qi, J.-L. Zhou, P. Li. Rapid Comm. Mass Spectrometry, 24, N 22 (2010) 3261—3270. https://doi.org/10.1002/rcm.4768
17. W. Tao, J. Duan, R. Zhao, X. Li, H. Yan, J. Li, Sh. Guo, N. Yang, Y. Tang. Food Chem., 141, N 3 (2013) 1681—1689, https://doi.org/10.1016/j.foodchem.2013.05.073
18. O. S. Chizhov, Yu. S. Ryabokobylko, A. V. Kessenikh. Russ. Chem. Bull., 28 (1979) 1482—1484, https://doi.org/10.1007/BF00947325
19. Kh. M. Bobokulov, M. G. Levkovich, A. Kh. Islamov, U. N. Zainutdinov, N. D. Abdullaev. Chem. Nat. Compd., 43, N 2 (2007) 149—152, https://doi.org/10.1007/s10600-007-0066-5
20. Z. I. Mavlyankulova, U. N. Zainutdinov, S. I. Mukhamedkhanova, V. B. Leont’ev, Kh. A. Aslanov. Khimiya Prirodnykh Soedinenii, N 1 (1979) 41—43
21. U. N. Zainutdinov, T. K. Yunusov, M. Dolmatov. Chem. Nat. Compd., 43, N 1 (2007) 66—71, https://doi.org/10.1007/s10600-007-0034-0
22. L. G. Vorontsova, O. S. Chizhov, B. L. Tarnopol’skii, V. I. Andrianov. Izv. Akad. Nauk SSSR, Ser. Khim., N 2 (1975) 338
23. S. A. Talipov, L. Yu. Izotova, B. Bekbulatova, B. T. Ibragimov, R. Islamov, U. N. Zainutdinov. Chem. Nat. Compd., 37, N 4 (2001) 322—324, https://doi.org/10.1023/A:1013710215954
24. A. Ibragimov, D. Dolimov, S. Talipov, L. Izotova, U. Zainutdinova. Acta Crystallograph. E: Crystallograph. Commun., 66, N 6 (2010) o1392, https://doi.org/10.1107/S1600536810017800
25. M. P. Nurmatova, U. N. Zainutdinov, F. G. Kamaev, Kh. A. Aslanov. Khimiya Prirodnykh Soedinenii, N 6 (1979) 788—792
26. U. N. Zainutdinov, M. P. Pulatova, T. A. Badalbaeva, R. U. Umarova, Z. I. Mavlyankulova, T. P. Pulatova, Kh. A. Aslanov. Chem. Nat. Compd., 30, N 1 (1994) 27—30, https://doi.org/10.1007/BF00638413
27. С. K. Hill, J. F. Hartwig. Nature Chem., 9, N 12 (2017) 1213—1221, https://doi.org/10.1038/nchem.2835
Review
For citations:
Baranovsky A.V., Sokolov S.N., Fatykhava S.A., Shabunya P.S., Esanov R.S., Tashpulatov F.N., Matchanov A.D. Spectral Analysis of Glycyrrhizic Acid, Lagochilin, Lagochirzine and Their Derivatives. Zhurnal Prikladnoii Spektroskopii. 2025;92(4):533-542. (In Russ.)
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